Synthesis and Characterization of Zeolite-A

Author


Ajeng Sekar Oktaviana Nugrahadianto(1Mail), Michelle Axelia Setio(2), Dewi Aulia Fadhilah(3),
(1) Department of Chemistry, Faculty of Science and Technology, Airlangga University,
(2) Department of Chemistry, Faculty of Science and Technology, Airlangga University,
(3) Department of Chemistry, Faculty of Science and Technology, Airlangga University,

Mail Corresponding Author
Article Analytic
  [File Size: 350KB]  Language: en
Available online: 2024-11-23  |  Published : 2024-11-23
Copyright (c) 2024 Ajeng Sekar Oktaviana Nugrahadia, Michelle Axelia Setio, Dewi Aulia Fadhilah
Article can trace at:

Article Metrics

Abstract Views: 73 times PDF Downloaded: 47 times

Abstract


Zeolite A is a material developed as a solution to the inconsistent crystallinity and impurities found in natural zeolites. It is a synthetic aluminosilicate that has numerous applications in catalysis, ion exchange, and molecular adsorption. This study aims to synthesize and characterize Zeolite A to explore its potential as an optimized synthetic zeolite. The synthesis process involved reacting sodium aluminate, sodium hydroxide, and tetraethyl orthosilicate (TEOS), followed by hydrothermal treatment, drying, and calcination to ensure complete crystallization. Characterization was performed using Fourier Transform Infrared Spectroscopy (FTIR) to identify structural bonds and gravimetric analysis to determine solid acidity. The synthesized Zeolite A has a yield of 61.08%. FTIR analysis confirmed the presence of aluminosilicate framework vibrations and the total solid acidity measured through gravimetric analysis is 2.9062 mmol/g. These results validate the effectiveness of the synthesis process, providing insights into the structural and acidic properties critical for industrial applications.


Keywords


Zeolite A, Zeolite Synthesis, FTIR, Solid Acidity

References


Atikah, W. S. 2017. The Potentiality of Activated Natural Zeolite From Gunung Kidul as Adsorbent to Textile Dyes. Arena Tekstil , 17-24.

Dar, Bashir Ahmad. 2019. Basic Concepts of Chemistry 1st Edition. Bookboon.com.

Dongoran, J., Sulistiawati, P., Simangunsong, S. Y., Paksi, P. G., & Pasaribu, M. H. 2021. Perkembangan Zeolit Sebagai Katalis Alam Potensial. Jurnal Jejaring Matematika dan Sains, Vol. 3 No. 2, 28-39.

Frost, R. L. and Johanson, U. 1998. Combination Bands In The Infrared Spectroscopy of Kaolins--A Drift Spectroscopic Study. Clays and Clay Minerals, 46, 466-477.

Kulprathlpanja S. 2010. Zeolites in Industrial Separation and Catalysis Weinheim: Wiley-VCH, 5(8), 19-24.

Nasar, M., & Salisu, N. 2014. Investigation of Effect of KBr Matrix on Drift Infrared Spectra of Some Minerals. ChemSearch Journal, 5(2), 14-19.

Saraswati, I. 2015. Zeolite-A Synthesis from Glass. Jurnal Sains dan Matematika, 23(4), 112-115.

Suwardi. (2009). Teknik Aplikasi Zeolit Di Bidang Pertanian Sebagai Bahan Pembenah Tanah. Jurnal Zeolit Indonesia, 8(1), 3338.

Tatsumi, T., 2004, Zeolites: Catalysis, Encyclopedia of Supramolecular Chemistry, 1: 1, 1610 -1616, Yokohama National University, Yokohama, Japan.

Valds, M. G., A.I.Perez-Cordoves, & Diaz-Garcia, M. 2006. Zeolites and zeolite-based materials in analytical chemistry. TrAC Trends in Analytical Chemistry, 24-30.


Refbacks

  • There are currently no refbacks.

Creative Commons License
This work is licensed under a Creative Commons Attribution-ShareAlike 4.0 International License.